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IEC 62321-11:2023 PDF

Determination of certain substances in electrotechnical products — Part 11: Tris (2-chloroethyl) phosphate (TCEP) in plastics by gas chromatography-mass spectrometry (GC-MS) and liquid chromatography-mass spectrometry (LC-MS)

First page of standard IEC 62321-11:2023Open preview (PDF)Determination of certain substances in electrotechnical products — Part 11: Tris (2-chloroethyl) phosphate (TCEP) in plastics by gas chromatography-mass spectrometry (GC-MS) and liquid chromatography-mass spectrometry (LC-MS)
Title (English):
IEC 62321-11:2023

Determination of certain substances in electrotechnical products — Part 11: Tris (2-chloroethyl) phosphate (TCEP) in plastics by gas chromatography-mass spectrometry (GC-MS) and liquid chromatography-mass spectrometry (LC-MS)

Document status:
Active
Format:
Electronic (PDF)
Number of pages:
67
Publication date:
December 20, 2023
Edition:
IEC IS 62321 edition 1 version 1
ICS:
13.020.01
Description (English):

This part of IEC 62321 specifies two different techniques for the determination of tris(2‑chloroethyl) phosphate (TCEP) in plastics, the GC-MS or LC-MS method, both of which are applicable to quantitative analysis. These two techniques are applicable to use with polyurethane, polyvinylchloride, and polyethylene materials containing TCEP between 200 mg/kg to 2 000 mg/kg. These test methods do not apply to plastic materials having a processing temperature higher than 230 °C. GC-MS using a pyrolyser/thermal desorption accessory (Py/TD-GC-MS) technique is described in REF _Ref141858781 \w \h Annex A 08D0C9EA79F9BACE118C8200AA004BA90B02000000080000000E0000005F005200650066003100340031003800350038003700380031000000 and can be used for the screening of TCEP in plastics. NOTE TCEP starts thermal decomposition at approximately 230 °C. Polymer types that have a processing temperature into shapes of plastics (e.g. pellets, moulded parts or sheets) not exceeding the decomposition temperature can contain TCEP.

Technical details

Technical committee
ISO/TC 61/SC 5 - Physical-chemical properties
SKU
IEC 62321-11:2023

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