ISO 15301:2001 PDF

Animal and vegetable fats and oils — Determination of sediment in crude fats and oils — Centrifuge method

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Title (English):

ISO 15301:2001

Animal and vegetable fats and oils — Determination of sediment in crude fats and oils — Centrifuge method

Document status:: Active
Format:: Electronic (PDF)
Number of pages:: 9
Publication date:: September 20, 2001
Edition:: ISO IS 15301 edition 1 version 1
ICS:: 67.200.10

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Description (English):

La présente Norme internationale spécifie une méthode pour la détermination de la teneur en sédiment dans des corps gras bruts susceptibles d'être séparés par la force centrifuge. Cette méthode est applicable aux corps gras bruts, ainsi qu'aux corps gras obtenus par extraction et/ou pression, dont la teneur en sédiment est comprise entre 0,03 ml par 100 g et 15 ml par 100 g. Cette méthode n'est pas applicable aux corps gras non liquides à une température de 20°C.

Technical details

Technical committee: ISO/TC 34/SC 11 - Animal and vegetable fats and oils
SKU: ISO 15301:2001

Abstract

Overview

ISO 15301:2001 specifies a rapid centrifuge method for the determination of sediment in crude animal and vegetable fats and oils. The method measures the volume of insoluble material that can be separated by centrifugal force and is applicable to crude oils (including oils from extraction and crushing) with sediment contents from 0.03 ml/100 g to 15 ml/100 g. It is not applicable to fats that are solid at 20 °C.

Key topics and technical requirements

Scope and definition: Sediment is the centrifugally separable portion of insoluble matter (e.g., phospholipids, impurities, particulate dirt) collected as an unclear layer at the bottom of the tube.
Sample preparation: Prepare test samples following ISO 661 and equilibrate to 20 °C ±2 to 5 °C. Redisperse any settled material before testing.
Apparatus:
- 100 ml pear- or cone-shaped glass centrifuge tubes with stoppers.
- Oil-resistant buckets and a centrifuge capable of delivering 700–800 × g at the narrow part of the tube (see Annex A for frequency calculation).
- Balance with 0.1 g readability.
Procedure:
- Weigh empty tubes, add 100 ml of test sample, re-weigh, centrifuge for 1 h at the specified relative acceleration.
- Read sediment volume: up to 1.5 ml with fine resolution (document specifies small-volume reading), volumes >1.5 ml to 0.5 ml resolution.
- Record centrifuge speed/acceleration (or swing diameter), and temperature before and after centrifuging.
Calculation and reporting:
- Sediment content w (ml/100 g) is calculated using the formula provided in the standard (based on sediment volume V and tube masses).
- Report mean of two tubes to the nearest 1 ml/100 g and include all test conditions in the report.
Precision:
- Repeatability and reproducibility limits are provided (e.g., for sediment

Related standards

Mentioned in the description and other ISO standards

Overview

Key topics and technical requirements

Scope and definition: Sediment is the centrifugally separable portion of insoluble matter (e.g., phospholipids, impurities, particulate dirt) collected as an unclear layer at the bottom of the tube.
Sample preparation: Prepare test samples following ISO 661 and equilibrate to 20 °C ±2 to 5 °C. Redisperse any settled material before testing.
Apparatus:
- 100 ml pear- or cone-shaped glass centrifuge tubes with stoppers.
- Oil-resistant buckets and a centrifuge capable of delivering 700–800 × g at the narrow part of the tube (see Annex A for frequency calculation).
- Balance with 0.1 g readability.
Procedure:
- Weigh empty tubes, add 100 ml of test sample, re-weigh, centrifuge for 1 h at the specified relative acceleration.
- Read sediment volume: up to 1.5 ml with fine resolution (document specifies small-volume reading), volumes >1.5 ml to 0.5 ml resolution.
- Record centrifuge speed/acceleration (or swing diameter), and temperature before and after centrifuging.
Calculation and reporting:
- Sediment content w (ml/100 g) is calculated using the formula provided in the standard (based on sediment volume V and tube masses).
- Report mean of two tubes to the nearest 1 ml/100 g and include all test conditions in the report.
Precision:
- Repeatability and reproducibility limits are provided (e.g., for sediment

ISO 15301:2001 PDF

Technical details

Abstract

Overview

Key topics and technical requirements

Related standards

Abstract

Overview

Key topics and technical requirements

Related standards

Animal and vegetable fats and oils. Preparation of test sample

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