ISO 5416:2006 PDF

Direct reduced iron — Determination of metallic iron — Bromine-methanol titrimetric method

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Title (English):

ISO 5416:2006

Direct reduced iron — Determination of metallic iron — Bromine-methanol titrimetric method

Document status:: Active
Format:: Electronic (PDF)
Number of pages:: 12
Publication date:: April 6, 2006
Edition:: ISO IS 5416 edition 3 version 1
ICS:: 73.060.10

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Description (English):

ISO 5416:2006 specifies a titrimetric method for the determination of the mass fraction of metallic iron in reduced iron ores (direct reduced iron: DRI). This method is applicable to mass fractions of metallic iron between 15 % and 95 % in DRI.

Technical details

Technical committee: ISO/TC 102/SC 2 - Chemical analysis
SKU: ISO 5416:2006

Abstract

Overview

ISO 5416:2006 specifies a bromine–methanol titrimetric method for the determination of the mass fraction of metallic iron in direct reduced iron (DRI). The procedure is applicable to DRI samples with metallic iron content between 15 % and 95 %. The standard describes sampling/preparation, required reagents and apparatus, the dissolution and titration procedure, calculation of results (including moisture correction and blank correction), and reporting requirements.

Key topics and technical requirements

Scope and applicability: Quantitative determination of metallic iron in DRI (15–95 % mass fraction).
Analytical principle: Metallic iron is dissolved with a freshly prepared bromine–methanol solution; insoluble residue is removed by filtration. Iron in the filtrate is reduced to Fe(II) and titrated with potassium dichromate after reduction with tin(II) chloride.
Reagents and solutions: Bromine–methanol (50 ml/l), hydrochloric and sulfuric acids, hydrogen peroxide, tin(II) chloride, mercury(II) chloride, iron standard, and potassium dichromate volumetric solution. Use analytical-grade reagents and water per ISO 3696.
Apparatus: Standard volumetric glassware (burette, pipettes, volumetric flasks), 100 ml conical flask, magnetic stirrer, and filtration with glass-fibre or microfilters (pore

Related standards

Mentioned in the description and other ISO standards

Overview

Key topics and technical requirements

Scope and applicability: Quantitative determination of metallic iron in DRI (15–95 % mass fraction).
Analytical principle: Metallic iron is dissolved with a freshly prepared bromine–methanol solution; insoluble residue is removed by filtration. Iron in the filtrate is reduced to Fe(II) and titrated with potassium dichromate after reduction with tin(II) chloride.
Reagents and solutions: Bromine–methanol (50 ml/l), hydrochloric and sulfuric acids, hydrogen peroxide, tin(II) chloride, mercury(II) chloride, iron standard, and potassium dichromate volumetric solution. Use analytical-grade reagents and water per ISO 3696.
Apparatus: Standard volumetric glassware (burette, pipettes, volumetric flasks), 100 ml conical flask, magnetic stirrer, and filtration with glass-fibre or microfilters (pore

ISO 5416:2006 PDF

Technical details

Abstract

Overview

Key topics and technical requirements

Related standards

Abstract

Overview

Key topics and technical requirements

Related standards

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