ISO 20263:2017 PDF

Microbeam analysis — Analytical electron microscopy — Method for the determination of interface position in the cross-sectional image of the layered materials

Title (English):

ISO 20263:2017

Microbeam analysis — Analytical electron microscopy — Method for the determination of interface position in the cross-sectional image of the layered materials

Document status:: Withdrawn
Format:: Electronic (PDF)
Number of pages:: 45
Publication date:: December 1, 2017
Edition:: ISO IS 20263 edition 1 version 1
ICS:: 37.020

Delivery type:

Full version25 €Read online 24h10 €Read online 72h15 €

Document language:

enru

Delivery time:Immediate download

Price:25 €

Description (English):

ISO 20263:2017 specifies a procedure for the determination of averaged interface position between two different layered materials recorded in the cross-sectional image of the multi-layered materials. It is not intended to determine the simulated interface of the multi-layered materials expected through the multi-slice simulation (MSS) method. This document is applicable to the cross-sectional images of the multi-layered materials recorded by using a transmission electron microscope (TEM) or a scanning transmission electron microscope (STEM) and the cross-sectional elemental mapping images by using an energy dispersive X-ray spectrometer (EDS) or an electron energy loss spectrometer (EELS). This document is also applicable to the digitized image recorded on an image sensor built into a digital camera, a digital memory set in the PC or an imaging plate and the digitalized image converted from an analogue image recorded on the photographic film by an image scanner.

Technical details

Technical committee: ISO/TC 202/SC 3 - Analytical electron microscopy
SKU: ISO 20263:2017

Abstract

Overview

ISO 20263:2017 - Microbeam analysis - Analytical electron microscopy - Method for the determination of interface position in the cross-sectional image of the layered materials - defines a standardized procedure to determine the averaged interface position between two layers in cross‑sectional images of multi‑layered materials. The method applies to images recorded with TEM or STEM and to elemental maps acquired with EDS or EELS, including digitized images from digital cameras, imaging plates or scanned photographic film. It is intended for practical thickness and interface evaluation (from a few nanometres to a few micrometres) and is explicitly not a substitute for atomic‑level multi‑slice simulation (MSS) methods.

Key Topics and Requirements

Scope & applicability
- Cross‑sectional TEM/STEM images and cross‑sectional elemental maps (EDS/EELS).
- Digitized image formats from CCD/CMOS cameras, imaging plates or scanners.
- Thickness range: from a few nm to a few μm.
Specimen preparation
- Cross‑section must be cut perpendicular to the layer stacking direction; cut angle required: 90° ± 6°.
- Typical thinning techniques: ultra‑microtomy, ion milling, FIB thinning, etc.
Image analysis workflow
- Define a region of interest (ROI) in the cross‑sectional image.
- Acquire an averaged intensity profile across the ROI (pixel intensity vs. distance).
- Apply moving‑averaged and differential processing to the intensity profile to detect averaged interface position.
- Use filtering/FFT as needed to manage noise and spatial frequency components.
Uncertainty & calibration
- Procedures for estimating uncertainty accumulated from specimen prep, imaging and image processing.
- Pixel‑size calibration (Annex C) and recommendations for reporting measurement uncertainty.
Limitations
- Not intended for determining atomically simulated interface positions from MSS (multi‑slice simulation).

Applications and Who Uses It

Materials scientists, electron microscopists, and metrology labs measuring layer thicknesses and interface flatness.
Semiconductor manufacturing, coatings and thin‑film industries, sensor development, and R&D groups needing repeatable, quantitative interface location from TEM/STEM images.
Useful for quality control, process verification, failure analysis and research where averaged interface position (not atomic registry) is required.

Related Standards

ISO 15932:2013 (methods referenced for FFT/IFFT concepts)
ISO 29301:2010 (definitions for digital imaging and detectors)
Additional ISO/TC 202 microbeam analysis guidance and terminologies

Keywords: ISO 20263:2017, microbeam analysis, analytical electron microscopy, TEM, STEM, EDS, EELS, interface position, cross-sectional imaging, ROI, image processing, moving average, differential processing, layer thickness.

Related standards

Mentioned in the description and other ISO standards

Abstract

Overview

Key Topics and Requirements

Scope & applicability
- Cross‑sectional TEM/STEM images and cross‑sectional elemental maps (EDS/EELS).
- Digitized image formats from CCD/CMOS cameras, imaging plates or scanners.
- Thickness range: from a few nm to a few μm.
Specimen preparation
- Cross‑section must be cut perpendicular to the layer stacking direction; cut angle required: 90° ± 6°.
- Typical thinning techniques: ultra‑microtomy, ion milling, FIB thinning, etc.
Image analysis workflow
- Define a region of interest (ROI) in the cross‑sectional image.
- Acquire an averaged intensity profile across the ROI (pixel intensity vs. distance).
- Apply moving‑averaged and differential processing to the intensity profile to detect averaged interface position.
- Use filtering/FFT as needed to manage noise and spatial frequency components.
Uncertainty & calibration
- Procedures for estimating uncertainty accumulated from specimen prep, imaging and image processing.
- Pixel‑size calibration (Annex C) and recommendations for reporting measurement uncertainty.
Limitations
- Not intended for determining atomically simulated interface positions from MSS (multi‑slice simulation).

Applications and Who Uses It

Materials scientists, electron microscopists, and metrology labs measuring layer thicknesses and interface flatness.
Semiconductor manufacturing, coatings and thin‑film industries, sensor development, and R&D groups needing repeatable, quantitative interface location from TEM/STEM images.
Useful for quality control, process verification, failure analysis and research where averaged interface position (not atomic registry) is required.

Related Standards

ISO 15932:2013 (methods referenced for FFT/IFFT concepts)
ISO 29301:2010 (definitions for digital imaging and detectors)
Additional ISO/TC 202 microbeam analysis guidance and terminologies

ISO 20263:2017 PDF

Technical details

Abstract

Overview

Key Topics and Requirements

Applications and Who Uses It

Related Standards

Related standards

Abstract

Overview

Key Topics and Requirements

Applications and Who Uses It

Related Standards

Related standards

Microbeam analysis — Analytical electron microscopy — Vocabulary

Microbeam analysis — Analytical transmission electron microscopy — Methods for calibrating image magnificatio…

Systems and software engineering — Software life cycle processes

Asset management — Vocabulary, overview and principles

Asset management — Asset management system — Requirements

Information technology — Radio frequency identification device conformance test methods — Part 2: Test method…

Information technology — Multimedia framework (MPEG-21) — Part 22: User Description

Milk — Determination of the lactoperoxidase activity — Photometric method (Reference method)